diff --git a/doc/news/add-kibler-2003-preparation.rst b/doc/news/add-kibler-2003-preparation.rst new file mode 100644 index 0000000..fe4dc33 --- /dev/null +++ b/doc/news/add-kibler-2003-preparation.rst @@ -0,0 +1,4 @@ +**Added:** + +* Added Au(100) and Au(110) in 0.1 M H2SO4 from kibler_2003_preparation. + diff --git a/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation.bib b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation.bib new file mode 100644 index 0000000..e6317e3 --- /dev/null +++ b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation.bib @@ -0,0 +1,6 @@ +@book{kibler_2003_preparation, + title = {Preparation and Characterisation of Noble Metal Single Crystal Electrode Surfaces}, + author = {Kibler, Ludwig A.}, + date = {2003}, + edition = {2nd edition}, +} diff --git a/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_dashed.svg b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_dashed.svg new file mode 100644 index 0000000..4b8bcbe --- /dev/null +++ b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_dashed.svg @@ -0,0 +1,157 @@ + + + + + + image-layer + + + + digitization-layer + + + j1: 125 A + + + + j2: -125 A + + + + E1: -0.6 V + + + + E2: 1.5 V + + scan rate: 10 mV / s + + curve: Au(100) dashed + + + + diff --git a/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_dashed.yaml b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_dashed.yaml new file mode 100644 index 0000000..e8d3293 --- /dev/null +++ b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_dashed.yaml @@ -0,0 +1,54 @@ +system: + type: electrochemical + electrolyte: + type: aqueous + components: + - name: H2O + type: solvent + proportion: + value: 100 + unit: volume percent + source: + refinement: Milli-Q + purity: + grade: ultrapure water + - name: H2SO4 + type: acid + source: + purity: + grade: ultrapure + concentration: + value: 0.1 + unit: mol L⁻¹ + ph: + value: 1.041 + comment: Estimated with CurTiPot on extraction from publication using a temperature of 25°C. + temperature: + value: 25 + unit: deg_C + comment: The electrolyte was at room temperature. + electrodes: + - name: REF + function: reference electrode + type: Hg/Hg2Cl2-sat + - name: CE + function: counter electrode + material: Pt + - name: WE + function: working electrode + material: Au + crystallographicOrientation: '100' + source: + manufacturer: MaTecK + shape: + type: cylinder +source: + citationKey: kibler_2003_preparation + url: https://www.uni-ulm.de/fileadmin/website_uni_ulm/nawi.inst.080/mitarbeiter/Kibler/KiblerSingleCrystals2003.pdf +curation: + process: + - role: curator + name: Johannes M. Hermann + orcid: https://orcid.org/0000-0001-7119-1295 + date: 2023-02-10 + diff --git a/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_solid.svg b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_solid.svg new file mode 100644 index 0000000..7406359 --- /dev/null +++ b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_solid.svg @@ -0,0 +1,157 @@ + + + + + + image-layer + + + + digitization-layer + + + curve: Au(100) solid + + + + j1: 125 A + + + + j2: -125 A + + + + E1: -0.6 V + + + + E2: 1.5 V + + scan rate: 10 mV / s + + diff --git a/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_solid.yaml b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_solid.yaml new file mode 100644 index 0000000..e8d3293 --- /dev/null +++ b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au100_solid.yaml @@ -0,0 +1,54 @@ +system: + type: electrochemical + electrolyte: + type: aqueous + components: + - name: H2O + type: solvent + proportion: + value: 100 + unit: volume percent + source: + refinement: Milli-Q + purity: + grade: ultrapure water + - name: H2SO4 + type: acid + source: + purity: + grade: ultrapure + concentration: + value: 0.1 + unit: mol L⁻¹ + ph: + value: 1.041 + comment: Estimated with CurTiPot on extraction from publication using a temperature of 25°C. + temperature: + value: 25 + unit: deg_C + comment: The electrolyte was at room temperature. + electrodes: + - name: REF + function: reference electrode + type: Hg/Hg2Cl2-sat + - name: CE + function: counter electrode + material: Pt + - name: WE + function: working electrode + material: Au + crystallographicOrientation: '100' + source: + manufacturer: MaTecK + shape: + type: cylinder +source: + citationKey: kibler_2003_preparation + url: https://www.uni-ulm.de/fileadmin/website_uni_ulm/nawi.inst.080/mitarbeiter/Kibler/KiblerSingleCrystals2003.pdf +curation: + process: + - role: curator + name: Johannes M. Hermann + orcid: https://orcid.org/0000-0001-7119-1295 + date: 2023-02-10 + diff --git a/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_dashed.svg b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_dashed.svg new file mode 100644 index 0000000..8295da6 --- /dev/null +++ b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_dashed.svg @@ -0,0 +1,157 @@ + + + + + + image-layer + + + + digitization-layer + + + j1: 75 A + + + + j2: -75 A + + + + E1: -0.6 V vs. SCE + + + + E2: 1.5 V vs. SCE + + + + curve: Au(110) dashed + + scan rate: 10 mV / s + + diff --git a/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_dashed.yaml b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_dashed.yaml new file mode 100644 index 0000000..0aa5038 --- /dev/null +++ b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_dashed.yaml @@ -0,0 +1,54 @@ +system: + type: electrochemical + electrolyte: + type: aqueous + components: + - name: H2O + type: solvent + proportion: + value: 100 + unit: volume percent + source: + refinement: Milli-Q + purity: + grade: ultrapure water + - name: H2SO4 + type: acid + source: + purity: + grade: ultrapure + concentration: + value: 0.1 + unit: mol L⁻¹ + ph: + value: 1.041 + comment: Estimated with CurTiPot on extraction from publication using a temperature of 25°C. + temperature: + value: 25 + unit: deg_C + comment: The electrolyte was at room temperature. + electrodes: + - name: REF + function: reference electrode + type: Hg/Hg2Cl2-sat + - name: CE + function: counter electrode + material: Pt + - name: WE + function: working electrode + material: Au + crystallographicOrientation: '110' + source: + manufacturer: MaTecK + shape: + type: cylinder +source: + citationKey: kibler_2003_preparation + url: https://www.uni-ulm.de/fileadmin/website_uni_ulm/nawi.inst.080/mitarbeiter/Kibler/KiblerSingleCrystals2003.pdf +curation: + process: + - role: curator + name: Johannes M. Hermann + orcid: https://orcid.org/0000-0001-7119-1295 + date: 2023-02-10 + diff --git a/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_solid.svg b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_solid.svg new file mode 100644 index 0000000..99b52e8 --- /dev/null +++ b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_solid.svg @@ -0,0 +1,112 @@ + + + + + image-layer + + + + digitization-layer + + + curve: Au(110) solid + + + + E1: -0.6 V vs. SCE + + + + E2: 1.5 V vs. SCE + + scan rate: 10 mV / s + + j2: 75 A + + + + j1: -75 A + + + + diff --git a/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_solid.yaml b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_solid.yaml new file mode 100644 index 0000000..0aa5038 --- /dev/null +++ b/literature/svgdigitizer/kibler_2003_preparation/kibler_2003_preparation_f5-2-1_Au110_solid.yaml @@ -0,0 +1,54 @@ +system: + type: electrochemical + electrolyte: + type: aqueous + components: + - name: H2O + type: solvent + proportion: + value: 100 + unit: volume percent + source: + refinement: Milli-Q + purity: + grade: ultrapure water + - name: H2SO4 + type: acid + source: + purity: + grade: ultrapure + concentration: + value: 0.1 + unit: mol L⁻¹ + ph: + value: 1.041 + comment: Estimated with CurTiPot on extraction from publication using a temperature of 25°C. + temperature: + value: 25 + unit: deg_C + comment: The electrolyte was at room temperature. + electrodes: + - name: REF + function: reference electrode + type: Hg/Hg2Cl2-sat + - name: CE + function: counter electrode + material: Pt + - name: WE + function: working electrode + material: Au + crystallographicOrientation: '110' + source: + manufacturer: MaTecK + shape: + type: cylinder +source: + citationKey: kibler_2003_preparation + url: https://www.uni-ulm.de/fileadmin/website_uni_ulm/nawi.inst.080/mitarbeiter/Kibler/KiblerSingleCrystals2003.pdf +curation: + process: + - role: curator + name: Johannes M. Hermann + orcid: https://orcid.org/0000-0001-7119-1295 + date: 2023-02-10 +